This operation is used to reduce the pressure of a vessel to a final pressure below ambient (1 atm, by default). If the final pressure must be equal or higher to the ambient pressure, please use a Venting operation, instead.
This operation may result in VOC emissions if volatile compounds are present in the vessel; for more details, see Chapter 10 (Emissions).
● Batch Vessel Procedure in a Reactor
● Batch Vessel Procedure in a Seed Reactor
● Batch Vessel Procedure in a Bioreactor
● Batch Vessel Procedure in a Seed Bioreactor
● Batch Vessel Procedure in a Disposable Bioreactor
● Batch Vessel Procedure in a Disposable Seed Bioreactor
● Batch Vessel Procedure in a Fermentor
● Batch Vessel Procedure in a Seed Fermentor
● Batch Vessel Procedure in a Disposable Bioreactor
● Inoculum Preparation Procedure in a Rocking Bioreactor
● Inoculum Preparation Procedure in a Roller Bottle
● Inoculum Preparation Procedure in a T-Flask
● Inoculum Preparation Procedure in a Shake Flask
● Inoculum Preparation Procedure in a Test Tube
● Nutsche Filtration Procedure
● Batch Distillation Procedure
● Batch Storage in a Blending Tank Procedure
● Batch Storage in a Flat Bottom Tank Procedure
● Batch Storage in a Receiver Tank Procedure
● Batch Storage in a Horizontal Tank Procedure
● Batch Storage in a Vertical-on-Legs Tank Procedure
● Batch Storage in a Drum Procedure
● Batch Storage in a Drum Procedure
● Batch Storage in a Tote Procedure
● Batch Storage in a Disposable Generic Container Procedure
● Batch 1x1 Generic Box Procedure
● Batch 3x3 Generic Box Procedure
● Batch 5x5 Generic Box Procedure
● Batch 10x10 Generic Box Procedure
The user specifies the final system pressure and the duration of this operation. The specified final pressure must be less than the initial pressure and less than the ambient pressure.
Note that the ambient pressure can be specified through the Reference Conditions dialog. To display this dialog, right-click on white space in the flowsheet and then select Reference Conditions... from the context menu that is displayed.
This operation affects the amount of gases in the freeboard space. The material balance calculations are done by assuming ideal gas behavior.
To account for the power consumption of the vacuum pump required to reduce the pressure from ambient to final, you may specify the vacuum pump power consumption through the Vent/Emissions tab, or you may click on the Setup button to open the Vacuum Pump Power Consumption Dialog and choose a different specification option for the vacuum pump power, such as the option to calculate the power consumption based on a suitable compression model.
In addition, you may specify a vacuum pump (as an auxiliary equipment) (optional) to account for the vacuum pump’s capital and operating costs and to consider the vacuum pump in scheduling calculations.
For more details, see Vacuum Pump Auxiliary Equipment Calculations.
The interface of this operation has the following tabs:
● Oper. Cond’s, see Evacuation: Oper. Conds Tab
● Vent/Emissions, see Vessel Operations: Vent/Emissions Tab
● Labor, etc, see Operations Dialog: Labor etc. Tab
● Description, see Operations Dialog: Description Tab
● Batch Sheet, see Operations Dialog: Batch Sheet Tab
● Scheduling, see Operations Dialog: Scheduling Tab